Potassium Hydroxide → Diepoxyoctane
反応式
[OH-:1].[K+].[CH2:3]1O[CH:4]1[CH2:6][CH2:7][CH2:8][CH2:9][CH:10]1[O:12][CH2:11]1>>[O:12]1[C:10]2([O:1][CH:11]12)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:4][CH3:3]参加物
3
実験手順
A 1-liter resin flask was charged with 200 g of PEG-7500 and 0.3 g KOH and vacuum stripped at 100° C. for one-half hour. To this stirred solution under nitrogen were added 5.5 g of 1,2,7,8-diepoxyoctane at 100° C. over 15 minutes. The mixture was maintained at this temperature for an additional one and one-half hours followed by quenching with 250 g of water.
後処理
- waitstripped at 100° C. for one-half hour
- temperatureThe mixture was maintained at this temperature for an additional one and one-half hours
- customby quenching with 250 g of water
出典と根拠
- ORDレコード
- ord-8891115a7a3b41ce8053755280664e69
- 出典データセット
- uspto-grants-1983_10
- 特許番号
- US04411775
反応ノート
読み込み中…