化工社化工社 化学情報印刷レポート · 研究参考用
p-Anisoyl chloride → HCID 13371227、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Anisoyl chloride | HCID 7477 | — |
| 反応物 | 1-(Morpholinocarbonylmethyl)piperazine | HCID 100622 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | HCID 13371227 | HCID 13371227 | — |
反応手順
10.25 g of piperazin-1-yl-acetic acid morpholide are cooled to 0° C. in 20 ml of methylene chloride. 8.75 g of anisoyl chloride are added dropwise in the course of 15 minutes. After the mixture has been subsequently stirred for 4 hours, it is diluted with isopropanol, whereupon the colourless product precipitates. It is filtered off with suction and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04610984 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-21ca3ae338254865a0d42275bcf052d1 |
| 出典メモ | uspto-grants-1986_09 |