Dimethyloctylamine → HCID 178419187、化合物
反応式
[CH2:1]([N:9]([CH3:11])[CH3:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[BH3:12].C(N(CC)CC)C>C(N(CC)CC)C>[BH3:12].[CH2:1]([N:9]([CH3:11])[CH3:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]参加物
4
実験手順
Octyldimethylamine (20.4 grams; 0.130 mole) was heated with triethylamine borane (1.9 grams; 0.130 mole) at reflux temperature until 12.8 grams (98%) of triethylamine had been collected in a cold trap. The reaction residue was distilled at reduced pressure to give N-octyl-N,N-dimethylamine borane boiling at 98°-100° C./0.9 mm. Hg. (19.6 grams; 89% yield).
後処理
- customhad been collected in a cold trap
- distillationThe reaction residue was distilled at reduced pressure
出典と根拠
- ORDレコード
- ord-d602c547b2d447c5a70a59f83b9251c5
- 出典データセット
- uspto-grants-1988_04
- 特許番号
- US04740504
反応ノート
読み込み中…