Hydrochloric Acid → 1,1-Cyclopentanedimethanamine

HRID 653082

反応式

HRID 653082 の反応式
Cl.Cl.[C:3]1([CH2:10][NH2:11])([CH2:8][NH2:9])[CH2:7][CH2:6][CH2:5][CH2:4]1.Cl>[OH-].[Na+].Cl[Pt-2](Cl)(Cl)Cl.[K+].[K+]>[C:3]1([CH2:10][NH2:11])([CH2:8][NH2:9])[CH2:7][CH2:6][CH2:5][CH2:4]1

参加物

5

反応物 2

HCID 313Hydrochloric AcidHCID 1317151911,1-Cyclopentanedimethanamine, dihydrochloride

生成物 1

HCID 4325931,1-Cyclopentanedimethanamine

試薬・触媒・溶媒 2

HCID 61440Dipotassium tetrachloroplatinate触媒HCID 14798Sodium Hydroxide溶媒

実験手順

A 2.01 g portion of this amine derivative was dissolved in 20 ml of 1N sodium hydroxide, the pH was adjusted to 7.0 with hydrochloric acid and 4.15 g of potassium tetrachloroplatinate was added. The mixture was stirred for 4 hours, then the solid was collected, washed with water and dried, giving 2.1 g of 1,1-cyclopentanedimethanamine, compound with platinum chloride.

後処理

  1. additionwas added
  2. customthe solid was collected
  3. washwashed with water
  4. customdried

出典と根拠

ORDレコード
ord-41bbad65c107481ba8ca2d3a2e78c1a2
出典データセット
uspto-grants-1987_06
特許番号
US04675336

関連ノート

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