Sodium Hydroxide → Sodium 2-chloro-3-benzyloxypropionate
反応式
[Cl:1][CH:2]([CH2:6][O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[C:3]([OH:5])=[O:4].[OH-].[Na+:16]>O>[Cl:1][CH:2]([CH2:6][O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[C:3]([O-:5])=[O:4].[Na+:16]参加物
4
実験手順
85 g of 2-chloro-3-benzyloxypropionic acid (0.396 mol) were suspended in 550 ml of water and neutralized to pH 7 with 10% sodium hydroxide. After stirring for 15 min, the resulting aqueous solution was washed with ethyl ether and evaporated to dryness under vacuum to give the desired compound.
後処理
- washthe resulting aqueous solution was washed with ethyl ether
- customevaporated to dryness under vacuum
出典と根拠
- ORDレコード
- ord-ce6d7bc3a6f446ad8c73792b287efab1
- 出典データセット
- uspto-grants-1992_07
- 特許番号
- US05132409
反応ノート
読み込み中…