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llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
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Methacrylic Acid → Ethyl acrylate methyl methacrylate

HRID 654875
ノート
印刷プレビュー

反応式

HRID 654875 の反応式
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[C:8]([O:13][CH3:14])(=[O:12])[C:9]([CH3:11])=[CH2:10].C(O)(=O)C(C)=C.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1.O.N>O.C(O)(C)C>[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[C:8]([O:13][CH3:14])(=[O:12])[C:9]([CH3:11])=[CH2:10]
参加物実験手順後処理出典と根拠反応ノート

参加物

8

反応物 5

HCID 4093Methacrylic AcidHCID 6658Methyl MethacrylateHCID 7187Benzoyl PeroxideHCID 8821Ethyl AcrylateHCID 12896473Azane;hydrate

生成物 1

HCID 62704Ethyl acrylate methyl methacrylate

試薬・触媒・溶媒 2

HCID 962
このページの内容参加物実験手順後処理出典と根拠反応ノート
Water
溶媒
HCID 3776Isopropanol溶媒

実験手順

To 150 g of isopropanol were added 55 g of ethyl acrylate, 35 g of methyl methacrylate and 10 g of methacrylic acid. To the resulting mixture was added 0.5 g of benzoyl peroxide, and thereafter, the mixture thus-obtained was subjected to polymerization reaction at 80° C. for 7 hours. Subsequently, 200 g of water and 4 g of 28% ammonia water were added thereto, and then, the isopropanol was completely removed by distillation to obtain an ethyl acrylate/methyl methacrylate copolymer.

後処理

  1. customthe mixture thus-obtained
  2. customwas subjected to polymerization reaction at 80° C. for 7 hours
  3. customthe isopropanol was completely removed by distillation

出典と根拠

ORDレコード
ord-1334f21ecacd496b96c85f1ba489d456
出典データセット
uspto-grants-1992_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US05134189

反応ノート

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