Dimethylethylamine → Dimethylethylammonium Trifluoromethanesulfonate

HRID 655089

反応式

HRID 655089 の反応式
[CH3:1][N:2]([CH3:5])[CH2:3][CH3:4].[F:6][C:7]([F:13])([F:12])[S:8]([OH:11])(=[O:10])=[O:9]>>[F:6][C:7]([F:13])([F:12])[S:8]([O-:11])(=[O:10])=[O:9].[CH3:1][NH+:2]([CH3:5])[CH2:3][CH3:4]

参加物

3

反応物 2

HCID 11723Dimethylethylamine2 回HCID 62406Trifluoromethanesulfonic acid2 回

生成物 1

HCID 86620366Dimethylethylammonium Trifluoromethanesulfonate

実験手順

Equimolar amounts of dimethylethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed dimethylethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

後処理

  1. temperaturewhile being cooled by liquid nitrogen
  2. customthus obtaining a target ionic conductor

出典と根拠

ORDレコード
ord-07047aba1c4045b6a58f03f746e70f9c
出典データセット
uspto-grants-2011_12
特許番号
US08071253B2

関連ノート

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