Triethylamine → Triethylammonium trifluoromethanesulfonate
反応式
[F:1][C:2]([F:8])([F:7])[S:3]([OH:6])(=[O:5])=[O:4].[CH2:9]([N:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH3:10]>>[F:1][C:2]([F:8])([F:7])[S:3]([O-:6])(=[O:5])=[O:4].[CH2:9]([NH+:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH3:10]参加物
3
実験手順
Equimolar amounts of triethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed triethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.
後処理
- temperaturewhile being cooled by liquid nitrogen
- customthus obtaining a target ionic conductor
出典と根拠
- ORDレコード
- ord-b1dbd61695ec42a4809475f3bb8c1881
- 出典データセット
- uspto-grants-2011_12
- 特許番号
- US08071253B2
反応ノート
読み込み中…