Water → Silver behenate

HRID 65548

反応式

HRID 65548 の反応式
[C:1]([OH:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].O.[N+]([O-])([O-])=O.[Ag+:30]>C1C=CC=CC=1>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Ag+:30]

参加物

5

反応物 3

HCID 962Water2 回HCID 8215Docosanoic AcidHCID 24470Silver Nitrate

生成物 1

HCID 164971Silver behenate

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

3.4 g of behenic acid was dissolved in 100 ml of benzene at 60° C., and the temperature of this solution was adjusted to 60° C. 100 ml of water was added to the above solution with stirring to form an emulsion. 100 ml of an aqueous solution of silver ammonium complex, which was prepared by adding aqueous to about 80 ml of an aqueous solution containing 1.7 g of silver nitrate, and then adding water to the aqueous solution to make the total volume one liter, was then added to the above emulsion. Crystallites of silver behenate were obtained.

後処理

  1. customwas adjusted to 60° C
  2. customto form an emulsion
  3. additionwas then added to the above emulsion

出典と根拠

ORDレコード
ord-bea4512df7a544c7832af1c2098a4279
出典データセット
uspto-grants-1978_12
特許番号
US04128428

関連ノート

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