Hydrochloric Acid → Benzenediazonium chloride

HRID 65551

反応式

HRID 65551 の反応式
[ClH:1].[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.Cl.[N:10]([O-])=O.[Na+]>O>[Cl-:1].[C:3]1([N+:2]#[N:10])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 8870Benzenamine hydrochloride (1:1)HCID 23668193Sodium Nitrite

生成物 1

HCID 60992Benzenediazonium chloride

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

A solution of benzenediazonium chloride was prepared as follows: To an ice cold (about 5° C.) solution of aniline hydrochloride (3.24 g., 25 mmoles) in water (10 ml.) and concentrated hydrochloric acid (2.1 ml., 25 mmoles) was added dropwise with stirring a solution of sodium nitrite (1.9 g., 27.5 mmoles) in water (10 ml.). After addition the solution was stirred in the cold for an additional 15 minutes.

後処理

  1. additionAfter addition the solution

出典と根拠

ORDレコード
ord-9a32150a3bf545fe94a430c25ee8ca32
出典データセット
uspto-grants-1978_12
特許番号
US04128425

関連ノート

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