Hydrochloric Acid → Benzenediazonium chloride
反応式
[ClH:1].[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.Cl.[N:10]([O-])=O.[Na+]>O>[Cl-:1].[C:3]1([N+:2]#[N:10])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1参加物
5
実験手順
A solution of benzenediazonium chloride was prepared as follows: To an ice cold (about 5° C.) solution of aniline hydrochloride (3.24 g., 25 mmoles) in water (10 ml.) and concentrated hydrochloric acid (2.1 ml., 25 mmoles) was added dropwise with stirring a solution of sodium nitrite (1.9 g., 27.5 mmoles) in water (10 ml.). After addition the solution was stirred in the cold for an additional 15 minutes.
後処理
- additionAfter addition the solution
出典と根拠
- ORDレコード
- ord-9a32150a3bf545fe94a430c25ee8ca32
- 出典データセット
- uspto-grants-1978_12
- 特許番号
- US04128425
反応ノート
読み込み中…