2-Cyclohexen-1-one, 2,5,6-trimethyl- → 2,3,6-Trimethylphenol
反応式
[CH3:1][C:2]1[C:3](=[O:10])[CH:4]([CH3:9])[CH:5]([CH3:8])[CH2:6][CH:7]=1>[Pd]>[CH3:9][C:4]1[C:5]([CH3:8])=[CH:6][CH:7]=[C:2]([CH3:1])[C:3]=1[OH:10]参加物
3
実験手順
1000 g of 2,5,6-trimethyl-2-cyclohexen-1-one is passed per hour per liter of catalyst at atmospheric pressure through an externally heated tube having a capacity of 250 cm3 and filled with a palladium/silica gel catalyst (0.2% by weight of palladium), the temperature being 300° C. The yield is 96% of 2,3,6-trimethylphenol. 4% of starting material is recovered and returned to the reaction.
後処理
- custombeing 300° C
出典と根拠
- ORDレコード
- ord-6c0e52ac2c3e41c5a1a9b2712864ce14
- 出典データセット
- uspto-grants-1978_12
- 特許番号
- US04128728
反応ノート
読み込み中…