Diazomethane → Methyl 3,5-Dibromobenzoate

HRID 658247

反応式

HRID 658247 の反応式
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([OH:7])=[O:6].[N+](=[CH2:14])=[N-]>CCOCC>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([O:7][CH3:14])=[O:6]

参加物

4

反応物 2

HCID 9550DiazomethaneHCID 12063Benzoic acid, 3,5-dibromo-

生成物 1

HCID 621923Methyl 3,5-Dibromobenzoate

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒2 回

実験手順

To a solution of 3,5-dibromobenzoic acid (1 eq.) in ether was added dropwise a solution of diazomethane in ether until gas evolution had ceased. The reaction was stirred for 20 min and concentrated in vacuo to afford the title compound.

後処理

  1. concentrationconcentrated in vacuo

出典と根拠

ORDレコード
ord-c9c0b78b58ea4da49f17993ef5b5aaae
出典データセット
uspto-grants-2011_12
特許番号
US08076359B2

関連ノート

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