2-(Trifluoromethyl)benzoic acid → 2-(Methylthio)-6-(trifluoromethyl)benzoic acid
反応式
CO[C:3]1[CH:11]=[C:10]([C:12]([F:15])([F:14])[F:13])[CH:9]=[C:8]([S:16][CH3:17])[C:4]=1C(O)=O.FC(F)(F)C1C=CC=CC=1[C:22]([OH:24])=[O:23].CSSC>>[CH3:17][S:16][C:8]1[CH:4]=[CH:3][CH:11]=[C:10]([C:12]([F:13])([F:14])[F:15])[C:9]=1[C:22]([OH:24])=[O:23]参加物
4
実験手順
The title compound, white solid, MS: m/e=235.0 [(M−H)−], was prepared in accordance with the general method of intermediate A from 2-(trifluoromethyl)benzoic acid and dimethyl disulfide.
出典と根拠
- ORDレコード
- ord-10dc0602ae0f4508b605142c6366b15d
- 出典データセット
- uspto-grants-2011_12
- 特許番号
- US08080541B2
反応ノート
読み込み中…