Sodium Hydroxide → Ampicillin Sodium

HRID 66053

反応式

HRID 66053 の反応式
[CH3:1][C:2]1([CH3:24])[S:6][C@@H:5]2[C@H:7]([NH:10][C:11]([C@H:13]([NH2:20])[C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=3)=[O:12])[C:8](=[O:9])[N:4]2[C@H:3]1[C:21]([OH:23])=[O:22].O.O.O.[OH-].[Na+:29]>O>[CH3:1][C:2]1([CH3:24])[S:6][C@@H:5]2[C@H:7]([NH:10][C:11]([C@H:13]([NH2:20])[C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=3)=[O:12])[C:8](=[O:9])[N:4]2[C@H:3]1[C:21]([O-:23])=[O:22].[Na+:29]

参加物

4

反応物 2

HCID 14798Sodium Hydroxide2 回HCID 23565Ampicillin Trihydrate

生成物 1

HCID 23663979Ampicillin Sodium

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

A suspension of 24.18 gm (60 millimols) of ampicillin trihydrate in 140 ml of water was admixed with 55.2 ml of an aqueous 1N sodium hydroxide solution (8% less than equimolar amount of NaOH) in the manner and under the conditions described in Example 1, and the sodium ampicillin was isolated in exactly the same manner as in Example 1.

出典と根拠

ORDレコード
ord-177c8f38f14b4e4d99132f91365c0976
出典データセット
uspto-grants-1978_12
特許番号
US04130558

関連ノート

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