反応式
P(Cl)(Cl)(Cl)(Cl)Cl.C(C(=C)C(O)=O)(=O)C1C=CC=CC=1.[Cl:20][C:21]1[CH:27]=[CH:26][CH:25]=[C:24]([Cl:28])[C:22]=1[NH2:23].[C:29]([CH:37]=[CH:38][C:39](NC1C(F)=C(F)C(F)=C(F)C=1F)=[O:40])(=[O:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1.FC1C(N)=C(F)C(F)=C(F)C=1F>>[C:29]([CH:37]=[CH:38][C:39]([NH:23][C:22]1[C:21]([Cl:20])=[CH:27][CH:26]=[CH:25][C:24]=1[Cl:28])=[O:40])(=[O:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1参加物
6
実験手順
The following additional compounds are prepared by employing PCl5 reagent in accordance with the method of the above Example 6. An analogous quantity of the appropriate benzoylacrylic acid or a substituted benzoylacrylic acid is employed in the manner of the benzoylacrylic acid of Example 5. Likewise, an analogous quantity of the appropriately substituted aniline is employed in the manner of the 2,6-dichloroaniline. Thus, to prepare 3-(benzoyl)pentafluoroacrylanilide, an analogous amount of benzoylacrylic acid is employed and there is used an analogous quantity of pentafluoroaniline in place of the 2,6-dichloroaniline.
後処理
- customThe following additional compounds are prepared
出典と根拠
- ORDレコード
- ord-3d7c09b7671b429ca9133e350ed4823e
- 出典データセット
- uspto-grants-1978_12
- 特許番号
- US04130661
関連ノート
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