4-Oxobutanoic acid → Isopropylaminium

HRID 66156

反応式

HRID 66156 の反応式
[O:1]=[CH:2][CH2:3][CH2:4][C:5]([OH:7])=[O:6].[CH:8]([NH2:11])([CH3:10])[CH3:9]>C1C=CC=CC=1>[CH:8]([NH3+:11])([CH3:10])[CH3:9].[O:1]=[CH:2][CH2:3][CH2:4][C:5]([O-:7])=[O:6]

参加物

5

反応物 2

HCID 11124-Oxobutanoic acidHCID 6363Isopropylamine

生成物 2

HCID 3364502IsopropylaminiumHCID 95432384-Oxobutanoate

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

100 Mg. of 4-(6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyric acid in 15 ml. of hot benzene is treated with 60 mg. of isopropyl amine. The solution is allowed to cool to room temperature and the product is filtered off, washed with ether and dried to yield isopropylammonium 4-(6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyrate.

後処理

  1. filtrationthe product is filtered off
  2. washwashed with ether
  3. customdried

出典と根拠

ORDレコード
ord-9fbbeabf522d4d0bb714410dabecfb77
出典データセット
uspto-grants-1978_12
特許番号
US04130654

関連ノート

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