2-Nitropropane → HCID 178430959、化合物

HRID 66957

反応式

HRID 66957 の反応式
[N+:1]([CH:4]([CH3:6])[CH3:5])([O-:3])=O.[CH:7]1[CH:15]=[CH:14][C:13]2[C:9](=[N:10][O:11][N+]=2[O-])[CH:8]=1.C(NCC)C>O1CCCC1>[CH3:5][C:4]1([CH3:6])[N+:1]([O-:3])=[C:13]2[CH:14]=[CH:15][CH:7]=[CH:8][C:9]2=[N+:10]1[O-:11]

参加物

5

反応物 3

HCID 3982-NitropropaneHCID 8021DiethylamineHCID 68075Benzofuroxan

生成物 1

HCID 178430959HCID 178430959、化合物

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

To a mixture containing 2-nitropropane (10.7 g., 0.12 moles), benzofuroxan (13.6 g., 0.10 moles) and tetrahydrofuran (50 ml.) is added dropwise diethylamine (8.7 g., 0.12 mole). The reaction temperature rises during addition. Upon completion of addition, the reaction mixture is allowed to sit overnight at room temperature.

後処理

  1. additionThe reaction temperature rises during addition
  2. additionUpon completion of addition

出典と根拠

ORDレコード
ord-1c8ab1a20a294172a812417cba9eb226
出典データセット
uspto-grants-1982_08
特許番号
US04343942

関連ノート

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