2-Nitropropane → HCID 178430959、化合物
反応式
[N+:1]([CH:4]([CH3:6])[CH3:5])([O-:3])=O.[CH:7]1[CH:15]=[CH:14][C:13]2[C:9](=[N:10][O:11][N+]=2[O-])[CH:8]=1.C(NCC)C>O1CCCC1>[CH3:5][C:4]1([CH3:6])[N+:1]([O-:3])=[C:13]2[CH:14]=[CH:15][CH:7]=[CH:8][C:9]2=[N+:10]1[O-:11]参加物
5
実験手順
To a mixture containing 2-nitropropane (10.7 g., 0.12 moles), benzofuroxan (13.6 g., 0.10 moles) and tetrahydrofuran (50 ml.) is added dropwise diethylamine (8.7 g., 0.12 mole). The reaction temperature rises during addition. Upon completion of addition, the reaction mixture is allowed to sit overnight at room temperature.
後処理
- additionThe reaction temperature rises during addition
- additionUpon completion of addition
出典と根拠
- ORDレコード
- ord-1c8ab1a20a294172a812417cba9eb226
- 出典データセット
- uspto-grants-1982_08
- 特許番号
- US04343942
反応ノート
読み込み中…