Isoprene → Isoprene sodium styrene sulfonate

HRID 703542ノート

反応式

HRID 703542 の反応式
[CH2:1]=[CH:2][C:3](=[CH2:5])[CH3:4].[CH:6]([S:14]([O-:17])(=[O:16])=[O:15])=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[Na+:18].C(S([O-])(=O)=O)CCCCCCCCCCC.[Na+].CCCCCCCCCCCCS.S(OOS([O-])(=O)=O)([O-])(=O)=O.[K+].[K+]>O>[CH2:1]=[CH:2][C:3](=[CH2:4])[CH3:5].[CH:6]([S:14]([O-:17])(=[O:15])=[O:16])=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[Na+:18]

参加物

7

反応物 5

HCID 6557IsopreneHCID 81951-DodecanethiolHCID 24412Potassium PersulfateHCID 23665726Sodium laurylsulfonateHCID 53627496Sodium styrenesulfonate

生成物 1

HCID 86744480Isoprene sodium styrene sulfonate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

In this example a copolymer emulsion of isoprene-sodium styrene sulfonate was prepared in the same way as that of Example 1, except the recipe and reaction conditions were somewhat different. In this example the reaction was carried out at 55° C. for five hours. The various ingredient quantities were as follows. Isoprene at 1020 grams, sodium styrene sulfonate 30 gms, water 1500 gms, sodium Lauryl sulfonate 75 gms, dodecylthiol 3.0 gms and potassium persulfate 3.75 gms. The sample of this run was identified as 172-D.

後処理

  1. customexcept the recipe and reaction conditions
  2. customwas carried out at 55° C. for five hours

出典と根拠

ORDレコード
ord-da43841d7b0f4f90b5c913d165fef86a
出典データセット
uspto-grants-1991_01
特許番号
US04983652

反応ノート

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