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HRID 709344作成日:2026年10月26日

Octane → Styrene

https://huagongshe.com/reaction/709344

反応式

関与物質

役割名称HCID仕込み量
反応物OctaneHCID 356—
反応物AzobisisobutyronitrileHCID 6547—
反応物StyreneHCID 7501—
溶媒WaterHCID 962—
生成物StyreneHCID 7501—
生成物p-DivinylbenzeneHCID 66041—

反応手順

1 g of the amphiphilic macromolecule reversible addition-fragmentation chain transfer agent and 80 g of deionized water were formulated into an aqueous solution as an aqueous phase, which was added and uniformly mixed with an oil phase consisting of 6 g of styrene, 12 g of p-vinyl benzene, 0.1 g of azobisisobutyronitrile and 9 g of n-octane, and prepared by an ultrasonic crasher into a miniemulsion under the effect of a high shear field. The miniemulsion was transferred to a reactor and subjected to the reaction at a temperature of 80° C. which stopped after 4 hours, and then cooled to the room temperature and discharged to yield polymeric nanocapsules with highly crosslinked shells which were formed by the polymerization of styrene and p-divinyl benzene, wherein the polymeric nanocapsules have an average diameter of 90 nm.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09180486B2
出典データセットuspto-grants-2015_11
ORD IDord-2e2acda0e6dc42248c0d402693e5079b
出典メモuspto-grants-2015_11