HRID709344

反应详情

EQUATION

反应方程式

HRID 709344 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1 g of the amphiphilic macromolecule reversible addition-fragmentation chain transfer agent and 80 g of deionized water were formulated into an aqueous solution as an aqueous phase, which was added and uniformly mixed with an oil phase consisting of 6 g of styrene, 12 g of p-vinyl benzene, 0.1 g of azobisisobutyronitrile and 9 g of n-octane, and prepared by an ultrasonic crasher into a miniemulsion under the effect of a high shear field. The miniemulsion was transferred to a reactor and subjected to the reaction at a temperature of 80° C. which stopped after 4 hours, and then cooled to the room temperature and discharged to yield polymeric nanocapsules with highly crosslinked shells which were formed by the polymerization of styrene and p-divinyl benzene, wherein the polymeric nanocapsules have an average diameter of 90 nm.

WORKUP

后处理

  1. additionwas added
  2. additionuniformly mixed with an oil phase
  3. customprepared by an ultrasonic crasher into a miniemulsion under the effect of a high shear field
  4. customThe miniemulsion was transferred to a reactor
  5. customsubjected to the reaction at a temperature of 80° C. which
  6. customto yield polymeric nanocapsules with highly crosslinked shells which