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(2-Methoxypyridin-4-yl)methanamine → 4-(Aminomethyl)pyridin-2(1H)-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2-Methoxypyridin-4-yl)methanamine | HCID 16227983 | — |
| 溶媒 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | 4-(Aminomethyl)pyridin-2(1H)-one | HCID 15079301 | — |
反応手順
The starting material (2-methoxypyridin-4-yl)methanamine 56-2 in 3N HCl was refluxed at 110° C. for 12 hours. The reaction was taken to dryness by rotary evaporation to give crude 4-(aminomethyl)pyridin-2(1H)-one 56-3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09181235B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-0a0113fcf18d4c1b932891df2d2f6d59 |
| 出典メモ | uspto-grants-2015_11 |