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HRID711263

反应详情

EQUATION

反应方程式

HRID 711263 的结构方程式

REACTANTS

反应物

1
结构：COc1cc(CN)ccn1
HCID16227983

1-(2-Methoxypyridin-4-yl)methanamine

C7H10N2O

PRODUCTS

生成物

1
结构：NCc1cc[nH]c(=O)c1
HCID15079301

4-(Aminomethyl)pyridin-2(1H)-one

C6H8N2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

The starting material (2-methoxypyridin-4-yl)methanamine 56-2 in 3N HCl was refluxed at 110° C. for 12 hours. The reaction was taken to dryness by rotary evaporation to give crude 4-(aminomethyl)pyridin-2(1H)-one 56-3.

WORKUP

后处理

  1. customThe reaction was taken to dryness by rotary evaporation