Diethyl Ether → HCID 22597223、化合物

HRID 7193

反応式

HRID 7193 の反応式
[CH3:1][C:2]1(O)[CH:9]2[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:11][CH:3]1[CH2:4]3)[CH2:8]2.[C:13](Cl)(=[O:16])[CH:14]=[CH2:15].C([O:20]CC)C>>[C:13]([O:16][C:3]12[CH2:11][CH:7]3[CH2:6][CH:5]([CH2:10][CH:9]([CH2:8]3)[CH:2]1[CH3:1])[CH2:4]2)(=[O:20])[CH:14]=[CH2:15]

参加物

4

反応物 3

HCID 3283Diethyl EtherHCID 13140Acryloyl chlorideHCID 1365452-Methyl-2-adamantanol

生成物 1

HCID 22597223HCID 22597223、化合物収率 55%

実験手順

200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).

後処理

  1. customThe reactant was reacted at room temperature for about 12 hours
  2. filtrationfiltered
  3. customSubsequently, the solvent was removed by an evaporator
  4. customthe reactant product was obtained
  5. distillationvacuum distillation (yield: 55%)

出典と根拠

ORDレコード
ord-36f2de1457284bf3b0fda06e472eab7b
出典データセット
uspto-grants-2006_08
特許番号
US07084227B2

関連ノート

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