化工社化工社 化学情報印刷レポート · 研究参考用
Cyanogen Bromide → 5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyanogen Bromide | HCID 10476 | — |
| 反応物 | o-Nitrobenzohydrazide | HCID 3781218 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine | HCID 712042 | — |
反応手順
4 ml of a 5M cyanogen bromide solution in acetonitrile were added dropwise to the solution of 3.6 g of 2-nitrobenzoic hydrazide in 20 ml of acetonitrile. This resulted first in a clear solution, then a solid precipitated out which was filtered off with suction after continuing to stir for a short time, washed again with acetonitrile and dried under reduced pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07138414B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-db67281e842a443a941f216a9cc75985 |
| 出典メモ | uspto-grants-2006_11 |