1-(3-Chlorophenyl)ethanone → Benzenemethanol, 3-chloro-alpha,alpha-dimethyl-
反応式
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]([CH3:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.[CH3:11][Mg]Br>O1CCCC1>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]([OH:9])([CH3:11])[CH3:10])[CH:5]=[CH:6][CH:7]=1参加物
4
実験手順
This compound is prepared in a manner analogous to that of Step A of this Example, using 13.9 grams (0.09 mole) of methyl 3-chlorophenyl ketone and 33.3 mL of methylmagnesium bromide (3.0M in diethyl ether) in 50 mL of dry tetrahydrofuran, yielding 2-(3-chlorophenyl)propan-2-ol.
後処理
- customThis compound is prepared in a manner analogous to that of Step A of this Example
出典と根拠
- ORDレコード
- ord-22495671f959406c98dda1a3261ec06e
- 出典データセット
- uspto-grants-1998_01
- 特許番号
- US05712281
反応ノート
読み込み中…