N,N-Dimethyltetradecylamine → Tetradecyldimethyl 2-acetyloxyethylammonium bromide

HRID 728383

反応式

HRID 728383 の反応式
[C:1]([O:4][CH2:5][CH2:6][Br:7])(=[O:3])[CH3:2].[CH2:8]([N:22]([CH3:24])[CH3:23])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>CC(CC)=O>[Br-:7].[CH2:8]([N+:22]([CH3:24])([CH3:23])[CH2:6][CH2:5][O:4][C:1](=[O:3])[CH3:2])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

参加物

4

反応物 2

HCID 8211N,N-DimethyltetradecylamineHCID 135641-Acetoxy-2-bromoethane

生成物 1

HCID 14625468Tetradecyldimethyl 2-acetyloxyethylammonium bromide

試薬・触媒・溶媒 1

HCID 6569Methyl Ethyl Ketone溶媒

反応条件

温度
90 °C

実験手順

In a reaction vessel was placed 42.8 grams of 2-bromoethyl acetate, 58.9 grams of tetradecyldimethylamine and 107.6 grams of methylethyl ketone (MEK) solvent. The mixtures was refluxed (ca. 90° C.) under nitrogen with stirring for 7 hours. The reaction mixture was cooled and the solvent decanted leaving as the product tetradecyldimethyl 2-acetyloxyethylammonium bromide.

後処理

  1. customIn a reaction vessel was placed
  2. temperatureThe reaction mixture was cooled
  3. customthe solvent decanted

出典と根拠

ORDレコード
ord-ecf0276c9b984c51ba50ff4b67327c1f
出典データセット
uspto-grants-1991_09
特許番号
US05047577

関連ノート

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