関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N,N-Dimethyltetradecylamine | HCID 8211 | — |
| 反応物 | 1-Acetoxy-2-bromoethane | HCID 13564 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | Tetradecyldimethyl 2-acetyloxyethylammonium bromide | HCID 14625468 | — |
反応手順
In a reaction vessel was placed 42.8 grams of 2-bromoethyl acetate, 58.9 grams of tetradecyldimethylamine and 107.6 grams of methylethyl ketone (MEK) solvent. The mixtures was refluxed (ca. 90° C.) under nitrogen with stirring for 7 hours. The reaction mixture was cooled and the solvent decanted leaving as the product tetradecyldimethyl 2-acetyloxyethylammonium bromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05047577 |
|---|
| 出典データセット | uspto-grants-1991_09 |
|---|
| ORD ID | ord-ecf0276c9b984c51ba50ff4b67327c1f |
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| 出典メモ | uspto-grants-1991_09 |
|---|
