huagongshe.com
HRID728383

反应详情

EQUATION

反应方程式

HRID 728383 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCCCCCCCN(C)C
HCID8211

Dimethyl(tetradecyl)amine

C16H35N

结构：CC(=O)OCCBr
HCID13564

ETHANOL, 2-BROMO-, ACETATE

C4H7BrO2

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCC[N+](C)(C)CCOC(C)=O.[Br-]
HCID14625468

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

In a reaction vessel was placed 42.8 grams of 2-bromoethyl acetate, 58.9 grams of tetradecyldimethylamine and 107.6 grams of methylethyl ketone (MEK) solvent. The mixtures was refluxed (ca. 90° C.) under nitrogen with stirring for 7 hours. The reaction mixture was cooled and the solvent decanted leaving as the product tetradecyldimethyl 2-acetyloxyethylammonium bromide.

WORKUP

后处理

  1. customIn a reaction vessel was placed
  2. temperatureThe reaction mixture was cooled
  3. customthe solvent decanted