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Deferoxamine Mesylate → Methanesulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Deferoxamine Mesylate | HCID 62881 | — |
| 反応物 | Manganese,4-pentanedionato-O,O')-, (OC-6-11)- | HCID 416789 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Methanesulfonate | HCID 85257 | — |
| 生成物 | HCID 131717012 | HCID 131717012 | — |
反応手順
With efficient stirring, 16.80 g (48 mmol) of manganese(III) acetylacetonate are added to 26.40 g (40 mmol) of desferrioxamine B mesylate in 400 ml of water and the mixture is efficiently stirred for 2 hours at room temperature. Working up as in Example 1 gives a deep green, slightly hygroscopic manganese(III) oxamine B mesylate that contains 0.5 mol of water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05051523 |
| 出典データセット | uspto-grants-1991_09 |
| ORD ID | ord-fd86185439964987af1df62a59085e5c |
| 出典メモ | uspto-grants-1991_09 |