Deferoxamine Mesylate → Methanesulfonate

HRID 729114Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 729114
C[C:2]([CH2:4][C:5]([CH3:7])=O)=[O:3].[CH3:8]C(CC(C)=O)=O.CC(CC(C)=O)=O.[Mn:22].CC(N(O)CCCCCNC(CCC(N(O)CCCCCNC(CCC(N(O)CCCCCN)=O)=O)=O)=O)=O.[CH3:62][S:63]([OH:66])(=[O:65])=[O:64]>O>[O:3]1[CH:2]=[CH:4][CH:5]=[CH:7][CH2:8]1.[Mn+3:22].[S:63]([O-:66])(=[O:65])(=[O:64])[CH3:62]

Komponenten

5

Edukt 2

HCID 62881Deferoxamine MesylateHCID 416789Manganese,4-pentanedionato-O,O')-, (OC-6-11)-

Produkt 2

HCID 85257MethanesulfonateHCID 131717012HCID 131717012, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

With efficient stirring, 16.80 g (48 mmol) of manganese(III) acetylacetonate are added to 26.40 g (40 mmol) of desferrioxamine B mesylate in 400 ml of water and the mixture is efficiently stirred for 2 hours at room temperature. Working up as in Example 1 gives a deep green, slightly hygroscopic manganese(III) oxamine B mesylate that contains 0.5 mol of water.

Quellen und Nachweise

ORD-Eintrag
ord-fd86185439964987af1df62a59085e5c
Quelldatensatz
uspto-grants-1991_09
Patentnummer
US05051523

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