化工社化工社 化学情報印刷レポート · 研究参考用
3-Chloro-4-nitrophenol → [2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-4-nitrophenol | HCID 10283 | — |
| 反応物 | 1-Chloro-2-(diethylamine)ethane hydrochloride | HCID 13363 | — |
| 溶媒 | Dichloromethane methanol | HCID 21226129 | — |
| 生成物 | [2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine | HCID 68816613 | — |
反応手順
Prepared analogously to Example 4.1.a. from 3-chloro-4-nitrophenol and (2-chloroethyl)diethylamine hydrochloride. Yield: 1.25 g (79.5% of theory); C12H17ClN2O3 (M=272.73); calc.: molecular ion peak (M+H)+: 273/275; found: molecular ion peak (M+H)+: 273/275; Rf value: 0.44 (silica gel, dichloromethane/methanol (90:10)).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07592373B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-0b2845645be14f609260747be85b6098 |
| 出典メモ | uspto-grants-2009_09 |