p-Toluidine → 4-ethyl-N-(4-methylphenyl)aniline

HRID 737267ノート

反応式

HRID 737267 の反応式
CCc1ccc(Br)cc1.Cc1ccc(N)cc1>CC(C)c1cc(C(C)C)c(-c2ccccc2[P](C2CCCCC2)(C2CCCCC2)->[Pd]2(<-[NH2]c3ccccc3-c3cccc[c]32)[O]S(=O)(=O)C(F)(F)F)c(C(C)C)c1.CCN=P(N=P(N(C)C)(N(C)C)N(C)C)(N(C)C)N(C)C.CS(C)=O.c1ccc(-c2ccno2)cc1>CCc1ccc(Nc2ccc(C)cc2)cc1

参加物

7

反応物 2

HCID 7813p-ToluidineHCID 153131-Bromo-4-ethylbenzene

生成物 1

HCID 208167124-ethyl-N-(4-methylphenyl)aniline収率 14.234%

試薬・触媒・溶媒 4

HCID 136800Isoxazole, 5-phenyl-試薬HCID 33931062,N'3,N'3,N3,N3,N'5,N'5,N5,N5-nonamethyl-2,4,6-triaza-3lambda5,5lambda5-diphosphaocta-3,5-diene-3,3,5,5-tetramine試薬HCID 178439018HCID 178439018、化合物触媒HCID 679Dimethyl Sulfoxide溶媒5 回

反応条件

温度
60 °C

実験手順

These solutions were added to a 384- well source plate (80 µL per well). The Mosquito HTS liquid handling robot was used to dose each of these solutions (200 nL each) into a 1536-well plate.

後処理

  1. addition手順は記録されていません

出典と根拠

ORDレコード
ord-49dd12992b7f465ea7b5c489a0d12acc
出典データセット
Ahneman

反応ノート

読み込み中…