2,2,2-Trifluoroethanol → Fluoroformic acid 2,2,2-trifluoroethyl ester

HRID 741528

反応式

HRID 741528 の反応式
[F:1][C:2]([F:6])([F:5])[CH2:3][OH:4].[C:7](F)([F:9])=[O:8]>>[C:2]([CH2:3][O:4][C:7]([F:9])=[O:8])([F:6])([F:5])[F:1]

参加物

3

反応物 2

HCID 64092,2,2-TrifluoroethanolHCID 9623Carbonyl fluoride

生成物 1

HCID 14493380Fluoroformic acid 2,2,2-trifluoroethyl ester

実験手順

236faE (CAS Reg. No. 20193-67-3) has been prepared by reaction of 2,2,2-trifluoroethanol with carbonyl fluoride to give the intermediate, CF3CH2OCOF, which was in turn reacted with sulfur tetrafluoride at 150°-200° C. to give the product as disclosed by Eisemann in U.S. Pat. No. 3,394,878.

出典と根拠

ORDレコード
ord-63b60552a7b74907b643503b04151a11
出典データセット
uspto-grants-1996_09
特許番号
US05552074

関連ノート

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