Ethyl 3-(naphthalen-2-yl)propanoate → 2-Naphthalenepropanol
反応式
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][CH2:12][C:13](OCC)=[O:14].[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][CH2:12][CH2:13][OH:14]参加物
4
実験手順
Following a procedure similar to that described in the first part of Preparation 4, the whole of this ethyl 3-(2-naphthyl)propionate was reacted with 668 mg of lithium aluminum hydride in tetrahydrofuran at room temperature for 1.5 hours. At the end of this time, the reaction mixture was worked up and purified as described in the first part of Preparation 4, to give 3.29 g of 3-(2-naphthyl)propanol as a colorless oil.
後処理
- customthat described in the first part of Preparation 4
- custompurified
- customas described in the first part of Preparation 4
出典と根拠
- ORDレコード
- ord-369aca6a51a94293a501737d7028e18b
- 出典データセット
- uspto-grants-1996_09
- 特許番号
- US05556864
反応ノート
読み込み中…