Methyl iodide → 131988-12-0

HRID 744593ノート

反応式

HRID 744593 の反応式
[CH3:1][I:2].[CH2:3]([O:5][C:6]1[C:7]([C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)=[N:8][S:9][N:10]=1)[CH3:4]>CC(C)=O>[I-:2].[CH2:3]([O:5][C:6]1[C:7]([C:11]2[CH:12]=[N+:13]([CH3:1])[CH:14]=[CH:15][CH:16]=2)=[N:8][S:9][N:10]=1)[CH3:4]

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 15180131Pyridine, 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)- (9CI)

生成物 1

HCID 15819042131988-12-0

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)pyridine (520 mg, 2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.72 g (83%).

後処理

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.72 g (83%)

出典と根拠

ORDレコード
ord-f2477284fe6f4ba09501daee37315841
出典データセット
uspto-grants-1996_09
特許番号
US05559138

反応ノート

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