Hydrochloric Acid → 1159010-32-8
反応式
[H][H].[CH3:3][CH:4]1[CH2:13][CH:12]2[CH:7]([CH2:8][CH2:9][CH2:10][CH2:11]2)[NH:6][CH2:5]1.[ClH:14]>CO.[Pt](=O)=O>[ClH:14].[CH3:3][CH:4]1[CH2:13][CH:12]2[CH:7]([CH2:8][CH2:9][CH2:10][CH2:11]2)[NH:6][CH2:5]1参加物
6
実験手順
In a hydrogen atmosphere 500 mg (3.5 mmol) 3-methyl-decahydro-quinoline, 75 mg platinum dioxide in 50 mL methanol and 3.5 mL 1M aqueous hydrochloric acid solution were hydrogenated at RT and 50 psi for 4 h. After removal of the catalyst by suction filtering the reaction mixture was evaporated down.
後処理
- customwere hydrogenated at RT
- customAfter removal of the catalyst by suction
- filtrationfiltering the reaction mixture
- customwas evaporated down
出典と根拠
- ORDレコード
- ord-b45247443a5b4997ad16ef0306794e9c
- 出典データセット
- uspto-grants-2014_09
- 特許番号
- US08829006B2
反応ノート
読み込み中…