Sodium borohydride → HCID 23310928、化合物
反応式
[BH4-].[Na+].[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH:12]=[O:13])([CH3:5])=[CH2:4]>C(O)(C)C>[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH2:12][OH:13])([CH3:5])=[CH2:4]参加物
4
実験手順
Into a 250 ml flask equipped with stirrer, thermometer reflux condensor, heating mantle and nitrogen blanket apparatus are placed 15 grams of sodium borohydride, 100 ml anhydrous isopropyl alcohol and 65 grams of 2-isopropenyl-1,5-dimethylcyclopentane carboxaldehyde having the structure: ##STR26## prepared according to U.S. Pat. No. 4,474,992 issued on Oct. 2, 1984.
後処理
- customInto a 250 ml flask equipped with stirrer
- temperaturethermometer reflux condensor, heating mantle and nitrogen blanket apparatus
- custom##STR26## prepared
出典と根拠
- ORDレコード
- ord-bb0f43f23f4b4f94ab1524f8c3e67002
- 出典データセット
- uspto-grants-1986_07
- 特許番号
- US04601850
反応ノート
読み込み中…