Hydrochloric Acid → Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride

HRID 747666

反応式

HRID 747666 の反応式
[C:1]([C:3]1[CH:13]=[CH:12][C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[CH:5][CH:4]=1)#[N:2].[ClH:14].[CH2:15]([OH:17])[CH3:16]>O1CCOCC1>[ClH:14].[CH2:15]([O:17][C:1]([C:3]1[CH:13]=[CH:12][C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[CH:5][CH:4]=1)=[NH:2])[CH3:16]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 81589Ethyl 4-cyanobenzoate

生成物 1

HCID 68830640Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride

試薬・触媒・溶媒 1

HCID 312751,4-Dioxane溶媒

実験手順

5.16 g (29 mmol) of ethyl 4-cyanobenzoate was stirred in 50 ml of 4N solution of hydrogen chloride in dioxane. 5 ml of ethanol was added to the resultant mixture, and they were stirred at room temperature for 4 days. The solvent was evaporated, and the residue was washed with ethyl acetate and dried to obtain the title compound.

後処理

  1. customThe solvent was evaporated
  2. washthe residue was washed with ethyl acetate
  3. customdried

出典と根拠

ORDレコード
ord-745c474fe6424adb93f48ea986009b47
出典データセット
uspto-grants-2008_07
特許番号
US07396844B1

関連ノート

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