化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Ethyl 4-(aminomethyl)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 4-(Aminomethyl)Benzoic Acid | HCID 65526 | — |
| 生成物 | Ethyl 4-(aminomethyl)benzoate | HCID 436161 | — |
反応手順
3 g (19.9 mmol) of 4-aminomethylbenzoic acid was suspended in 100 ml of ethanol. 10 ml of ethanol containing 25% of hydrogen chloride was added to the suspension, and they were heated under reflux for 8 hours. The solvent was evaporated, and the title compound was obtained by the same isolation process as that of step 1 in Example 1 with ethyl acetate as the extractant.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07396844B1 |
| 出典データセット | uspto-grants-2008_07 |
| ORD ID | ord-87b785d9a67d48c78c90f7eb6d0262e3 |
| 出典メモ | uspto-grants-2008_07 |