Isobutyraldehyde → 1-(1-Benzyl-1H-1,2,4-triazol-5-yl)-2-methylpropan-1-ol

HRID 748063

反応式

HRID 748063 の反応式
[C:1]1([CH2:7][N:8]2[CH:12]=[N:11][CH:10]=[N:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:13](=[O:17])[CH:14]([CH3:16])[CH3:15]>>[CH2:7]([N:8]1[C:12]([CH:13]([OH:17])[CH:14]([CH3:16])[CH3:15])=[N:11][CH:10]=[N:9]1)[C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

参加物

3

反応物 2

HCID 6561IsobutyraldehydeHCID 224581-(Phenylmethyl)-1H-1,2,4-triazole

生成物 1

HCID 685956691-(1-Benzyl-1H-1,2,4-triazol-5-yl)-2-methylpropan-1-ol収率 71%

実験手順

1-(1-Benzyl-1H-1,2,4-triazol-5-yl)-2-methylpropan-1-ol was synthesized in a manner similar to that of procedure 21 B but using 1-(phenylmethyl)-1H-1,2,4-triazole and isobutyraldehyde as the starting materials. The product was isolated as a white solid in 71% yield.

後処理

  1. customThe product was isolated as a white solid in 71% yield

出典と根拠

ORDレコード
ord-e37f5d0e8162451bb1c32fe29e6c0a00
出典データセット
uspto-grants-2008_07
特許番号
US07399778B2

関連ノート

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