HCID 22939353、化合物 → HCID 59750359、化合物
反応式
C([O:8][C:9]1[N:14]=[C:13]([C:15]2[S:16][C:17]3[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=3[C:19](=[O:21])[N:20]=2)[CH:12]=[CH:11][CH:10]=1)C1C=CC=CC=1>FC(F)(F)C(O)=O>[O:8]=[C:9]1[NH:14][C:13]([C:15]2[S:16][C:17]3[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=3[C:19](=[O:21])[N:20]=2)=[CH:12][CH:11]=[CH:10]1参加物
3
実験手順
2-(6-(Benzyloxy)-2-pyridyl)-4H-1,3-benzothiazine-4-one (0.15 g, 0.43 mmol) was dissolved in trifluoroacetic acid (10 ml), and the mixture was stirred at room temperature for 15 hrs. The solvent was evaporated, and the residue was recrystallized from chloroform-hexane to give the titled compound (0.07 g, 69%).
後処理
- customThe solvent was evaporated
- customthe residue was recrystallized from chloroform-hexane
出典と根拠
- ORDレコード
- ord-92b954082ba34b7cac39b11d24dfaca4
- 出典データセット
- uspto-grants-2008_07
- 特許番号
- US07399759B2
反応ノート
読み込み中…