4-Methoxybenzenesulfonamide → HCID 178492905、化合物
反応式
COc1ccc(S(N)(=O)=O)cc1.O=C(O)c1ccnc(C(F)(F)F)c1.C1CCC(CC1)N=C=NC2CCCCC2.C1CC(=O)N(C1=O)O.CN1CCOCC1.CN(C)C=O>>COc1ccc(S(=O)(=O)NC(=O)c2ccnc(C(F)(F)F)c2)cc1参加物
7
反応条件
- 温度
- 25 °C
後処理
- addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
- addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
- aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
- addition380 uL MeCN solvent were added to the transfer plate
- aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
- addition180 uL MeCN added to filter plate 1 for LCMS analysis
- aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
- addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
- customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM
出典と根拠
- ORDレコード
- ord-81706c11bfe2475fadcdb786c533ad9d
- 出典データセット
- AIChemEco amide coupling conditions 47k dataset
反応ノート
読み込み中…