反応式
[CH3:1][C:2]([CH3:7])([CH3:6])[CH2:3][CH:4]=O.[O:8]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][NH2:16])[CH2:10][CH2:9]1.[S-:17][C:18]#[N:19].[K+].II>>[C:2]([C:3]1[S:17][C:18](=[NH:19])[N:16]([CH2:15][CH2:14][N:11]2[CH2:12][CH2:13][O:8][CH2:9][CH2:10]2)[CH:4]=1)([CH3:7])([CH3:6])[CH3:1]参加物
5
実験手順
Commercially available 3,3-dimethylbutanal (Aldrich), 2-morpholinoethanamine (Aldrich), potassium thiocyanate (Aldrich) and iodine (EMD chemicals) were processed using the method described in Example 315A to afford the title compound. MS (ESI+) m/z 270 (M+H)+.
出典と根拠
- ORDレコード
- ord-20bf1fd02fb3407f909fd7192f51f7fa
- 出典データセット
- uspto-grants-2014_09
- 特許番号
- US08841334B2
関連ノート
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