Hydrochloric Acid → HCID 131730803、化合物

HRID 83823

反応式

HRID 83823 の反応式
[CH3:1][N:2]1[C:7]2=[N:8][CH2:9][CH2:10][CH2:11][N:6]2[CH2:5][CH2:4][CH2:3]1.[ClH:12]>CCOCC>[ClH:12].[CH3:1][N:2]1[C:7]2=[N:8][CH2:9][CH2:10][CH2:11][N:6]2[CH2:5][CH2:4][CH2:3]1

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 1235837-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene

生成物 1

HCID 131730803HCID 131730803、化合物

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

A flame dried flask was charged with MTBD (0.25 g, 1.63 mmol), ether (10 mL) and a stirbar under dry nitrogen atmosphere. With vigorous stirring a 1M ethereal HCl solution (1.6 mL) was then added to form a white precipitate. Stirring was continued for 1 hour then excess solvent was decanted to yield 0.29 g (94%). The salt was then dried under high vacuum.

後処理

  1. customA flame dried flask
  2. additionwas then added
  3. customto form a white precipitate
  4. customexcess solvent was decanted
  5. customto yield 0.29 g (94%)
  6. customThe salt was then dried under high vacuum

出典と根拠

ORDレコード
ord-e12c52601aad40bdbaaefe1cc77a32ec
出典データセット
uspto-grants-2014_09
特許番号
US08846851B2

関連ノート

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