Hydrochloric Acid → 1-(1-Chloroethyl)-3-methoxybenzene

HRID 839393

反応式

HRID 839393 の反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9](O)[CH3:10])[CH:6]=[CH:7][CH:8]=1.[ClH:12]>O>[Cl:12][CH:9]([C:5]1[CH:6]=[CH:7][CH:8]=[C:3]([O:2][CH3:1])[CH:4]=1)[CH3:10]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 90902(+-)-1-(3-Methoxyphenyl)ethanol

生成物 1

HCID 128614131-(1-Chloroethyl)-3-methoxybenzene

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Into a solution of 152.1 g (1 mol) of 1-(3'-methoxyphenyl)-ethan-1-ol in 750 ml petroleum ether, one introduces hydrogen chloride during ice cooling until water separation is completed. The organic phase is then washed with ice-cold water, dried and the petroleum ether is removed in vacuo. The thermo-labile residue is used without any further purification.

後処理

  1. washThe organic phase is then washed with ice-cold water
  2. customdried
  3. customthe petroleum ether is removed in vacuo
  4. customThe thermo-labile residue is used without any further purification

出典と根拠

ORDレコード
ord-741b9bf5f4a34758aa2a5e85ba27fdb7
出典データセット
uspto-grants-1978_06
特許番号
US04094994

関連ノート

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