Butyl Acrylate → alpha-Methylene-gamma-butyrolactone n-butyl acrylate acrylic acid

HRID 83947

反応式

HRID 83947 の反応式
[CH2:1]=[C:2]1[CH2:7][CH2:6][O:5][C:3]1=[O:4].[C:8]([O:12][CH2:13][CH2:14][CH2:15][CH3:16])(=[O:11])[CH:9]=[CH2:10]>>[CH2:1]=[C:2]1[CH2:7][CH2:6][O:5][C:3]1=[O:4].[C:8]([O:12][CH2:13][CH2:14][CH2:15][CH3:16])(=[O:11])[CH:9]=[CH2:10].[C:3]([OH:5])(=[O:4])[CH:2]=[CH2:1]

参加物

3

実験手順

Similar to Example 51, with the following exception: 3.390 g (3.46×10−2 mol) α-methylene-γ-butyrolactone and 1.075 g (8.39×10−3 mol) n-butyl acrylate were used in the monomer mixture, yielding a polymer with a glass transition temperature of 145° C. Comparison to the Fox equation suggests the statistical copolymer contains approximately 11% n-butyl acrylate repeat units.

後処理

  1. customyielding a polymer with a glass transition temperature of 145° C

出典と根拠

ORDレコード
ord-01b081e27a914390b17b8bb8f541974c
出典データセット
uspto-grants-2014_09
特許番号
US08846817B2

関連ノート

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