HCID 178478098、化合物 → HCID 178420213、化合物
反応式
Cl[C:2]1[CH:7]=[CH:6][CH:5]=[C:4](Cl)[C:3]=1[CH2:9][C:10]1[NH:14][N:13]=[N:12][N:11]=1>[Pd].CO>[C:3]1([CH2:9][C:10]2[NH:14][N:13]=[N:12][N:11]=2)[CH:2]=[CH:7][CH:6]=[CH:5][CH:4]=1参加物
4
実験手順
The mixture of 5-(2,6-dichlorophenylmethyl)tetrazole (355 mg), 5% palladium on activated carbon (93 mg) and methanol (8 ml) was stirred for 1 h room temperature under an atmosphere of hydrogen gas. The reaction mixture was filtered through Celite (trade mark) and the filtrate was concentrated to give the title compound having the following physical data.
後処理
- filtrationThe reaction mixture was filtered through Celite (trade mark)
- concentrationthe filtrate was concentrated
出典と根拠
- ORDレコード
- ord-dbca2720337a4c9a98eaadeb62c55c46
- 出典データセット
- uspto-grants-2002_04
- 特許番号
- US06376484B1
反応ノート
読み込み中…