2-(2-Methylethyl)-6-methylbenzoic acid → HCID 69336578、化合物

HRID 844853

反応式

HRID 844853 の反応式
C[O:2][C:3](=[O:24])[C@H:4]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([C:13]2[C:14](=[O:23])[N:15]([CH3:22])[C:16](=[O:21])[N:17]([CH3:20])[C:18]=2[CH3:19])=[CH:9][CH:8]=1)[NH2:5].[CH3:25][CH2:26][CH2:27][C:28]1[CH:36]=[CH:35][CH:34]=[C:33]([CH3:37])[C:29]=1[C:30](O)=[O:31]>>[CH3:25][CH2:26][CH2:27][C:28]1[CH:36]=[CH:35][CH:34]=[C:33]([CH3:37])[C:29]=1[C:30]([NH:5][C@H:4]([C:3]([OH:2])=[O:24])[CH2:6][C:7]1[CH:8]=[CH:9][C:10]([C:13]2[C:14](=[O:23])[N:15]([CH3:22])[C:16](=[O:21])[N:17]([CH3:20])[C:18]=2[CH3:19])=[CH:11][CH:12]=1)=[O:31]

参加物

3

反応物 2

HCID 226137482-(2-Methylethyl)-6-methylbenzoic acidHCID 693369754-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester

生成物 1

HCID 69336578HCID 69336578、化合物

実験手順

N-[[2-(2-methylethyl)-6-methylphenyl]carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2-(2-methylethyl)-6-methylbenzoic acid using the general procedures described in example 7 and was obtained as an amorphous white solid. ES-HRMS m/e calcd for C27H31N3O5 (M+Na) 500.2156, found 500.2160.

後処理

  1. customwas obtained as an amorphous white solid

出典と根拠

ORDレコード
ord-c92b869201b54800aba333425698294b
出典データセット
uspto-grants-2002_04
特許番号
US06380387B1

関連ノート

読み込み中…