化工社化工社 化学情報印刷レポート · 研究参考用
2,6-Difluorobenzoic acid → CH9Z955RV6
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Difluorobenzoic acid | HCID 9796 | — |
| 反応物 | 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester | HCID 69336975 | — |
| 生成物 | CH9Z955RV6 | HCID 69337579 | — |
反応手順
N-[(2,6-difluorophenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2,6-difluorobenzoic acid using the general procedures described in example 7 and was obtained as an amorphous white solid. ES-HRMS m/e calcd for C23H21F2N3O5 (M+Na) 480.1483, found 480.1489.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06380387B1 |
| 出典データセット | uspto-grants-2002_04 |
| ORD ID | ord-9d97a366f3834445923236b2b29e754e |
| 出典メモ | uspto-grants-2002_04 |