HCID 54084144、化合物 → HCID 18800733、化合物
反応式
[C:1]1([CH:7]=[CH:8][CH2:9][CH:10]2[NH:16][C:15](=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>CO.[Pd]>[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]2[NH:16][C:15](=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1参加物
4
実験手順
The title material of Example 32 (0.46 g, 2.0 mmol) in MeOH and 4% Pd on carbon (0.10 g) were combined in a standard Parr apparatus (125 mL bottle). The hydrogenation was carried out at room temperature under a H2 pressure of 5 psi for 1 hr. All solvent was then removed under reduced pressure to yield 0.50 (09%) of the title material as a white semi-solid.
後処理
- customwas carried out at room temperature under a H2
- customfor 1 hr
- customAll solvent was then removed under reduced pressure
出典と根拠
- ORDレコード
- ord-f0a888963ef647c2b390f93c16c48191
- 出典データセット
- uspto-grants-2000_01
- 特許番号
- US06011028
反応ノート
読み込み中…